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Statistical analyses As Pearson correlation coefficients between the nine metabolite concentration values (three metabolites in three voxels) were substantial even after adjustment for potential confounders, we used principal component analysis (PCA) to identify latent metabolite variables, and extracted scores for each component (see Results and SA7 for details)

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The RI and MALS signals were used to detect the eluting complex and to deduce its absolute molecular mass using an algorithm implemented in the ASTRA 6.0 software package (Wyatt Technology)